Home > Organosilicon Compounds> [(2R,3S,4R,5R,6S)-3,4-diacetyloxy-5-azido-6-[tert-butyl(dimethyl)silyl]oxyoxan-2-yl]methyl acetate

[(2R,3S,4R,5R,6S)-3,4-diacetyloxy-5-azido-6-[tert-butyl(dimethyl)silyl]oxyoxan-2-yl]methyl acetate

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Origin: China

Cas No: 99049-65-7

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 80 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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CAS No.: 99049-65-7 Formula: C12H25N3O5Si Molecular Weight: 319.43000

Basic Info

Chemical Name	[(2R,3S,4R,5R,6S)-3,4-diacetyloxy-5-azido-6-[tert-butyl(dimethyl)silyl]oxyoxan-2-yl]methyl acetate
Synonyms	t-Butyldimethylsilyl-2-azido-2-deoxy-3,4,6 tri-O-acetyl b-D-glucopyranose; 1-O-tert-Butyldimethylsilyl 2-azido-2-deoxy-\|A-D-glucopyranoside 3,4,6-triacetate;
CAS No.	99049-65-7
Molecular Formula	C12H25N3O5Si
Molecular Weight	319.43000
PSA	128.90000
LogP	0.57886

Properties

Melting Point	66-70 °C(lit.)

Synthesis Route

1H-imidazole+2-azido-2-deoxy-3,4,6-tri-O-acetyl-α,β-D-glucopyranosyl acetate→[(2R,3S,4R,5R,6S)-3,4-diacetyloxy-5-azido-6-[tert-butyl(dimethyl)silyl]oxyoxan-2-yl]methyl acetate
2-azido-2-deoxy-3,4,6-tri-O-acetyl-α,β-D-glucopyranosyl acetate→[(2R,3S,4R,5R,6S)-3,4-diacetyloxy-5-azido-6-[tert-butyl(dimethyl)silyl]oxyoxan-2-yl]methyl acetate
(2R,3S,4R)-2-(acetoxymethyl)-5-azido-6-(nitrooxy)tetrahydro-2H-pyran-3,4-diyl diacetate→[(2R,3S,4R,5R,6S)-3,4-diacetyloxy-5-azido-6-[tert-butyl(dimethyl)silyl]oxyoxan-2-yl]methyl acetate

Precursor

2-azido-2-deoxy-3,4,6-tri-O-acetyl-α,β-D-glucopyranosyl acetate
tert-butyldimethylsilyl chloride
1H-imidazole
[(2R,3S,4R)-3,4-diacetyloxy-3,4-dihydro-2H-pyran-2-yl]methyl acetate

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