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N,N-Dimethylformamide dimethyl acetal

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Origin: China

Cas No: 4637-24-5

Specification: 99%min

Min order Quantity: 1 /kg

Supply Ability: 50 mt/month

Lead time: 7 days for OEM, 3 days for ready goods

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Products Specification
Product Description

Quick Details
CAS No.:
4637-24-5
Other Names:
N,N-Dimethylformamide dimethyl acetal
MF:
C5H13NO2
EINECS No.:
225-063-3
Type:
Pharmaceutical Intermediates, Syntheses Material Intermediates
Purity:
98%
Application:
API
Appearance:
White to off-white
Test Method:
HPLC Test
Other Country:
Shaanxi
Packaging&Delivery
Packaging Details
Packing:1kg/bad,25kgs/drum Two plasti-bags inside and Paper-drums or as customer's requirements
Port
Major ports in China
Lead Time:
Quantity(Grams) 1 - 10000 >10000
Est. Time(days) 1 To be negotiated

Property

CAS No.: 4637-24-5 Formula: C5H13NO2 Molecular Weight: 119.16200

Description

1,1-Dimethoxy-N,N-dimethylmethanamine is used as a reagent in the formation of pyridine derivatives that exhibit inhibition against PI3 kinase p110α enzymes.

Basic Info

Chemical Name	N,N-Dimethylformamide dimethyl acetal
Synonyms	DMF-DMA; DMF-Dimethyl acetal; 1,1-Dimethoxy-N,N-dimethylmethanamine; Methanamine, 1,1-dimethoxy-N,N-dimethyl-; 1,1-Dimethoxy-N,N-dimethylmethylamine; 1,1-Dimethoxytrimethylamine;
CAS No.	4637-24-5
Molecular Formula	C5H13NO2
Molecular Weight	119.16200
PSA	21.70000
LogP	0.12440

Properties

Appearance & Physical State	Clear, colorless liquid.
Density	0.897
Boiling Point	104-108ºC
Melting Point	-85ºC
Flash Point	7ºC
Refractive Index	1.3972
Water Solubility	hydrolysis
Stability	Stable under normal temperatures and pressures.
Storage Condition	Flammables area

Safety Info

Hazard Class	3
Safety Statements	S16-S26-S36/37/39
HS Code	29225000
WGK Germany	1
Packing Group	II
RIDADR	UN 3271
Risk Statements	R11; R20; R36/38
Hazard Codes	F; Xn
Signal Word	Danger
Symbol	GHS02, GHS07
Caution Statement	P210; P261; P280; P304 + P340 + P312; P305 + P351 + P338; P370 + P378
Hazard Declaration	H225; H315; H317; H319; H332; H335

Synthesis Route

methyl 2-((31S,6aR,9aR)-9-oxooctahydro-4H-pyrrolo[3,2,1-ij]quinolin-6a(31H)-yl)acetate+benzyl (3aR,7R)-7-(4-hydrazineyl-2,3-dimethoxyphenyl)-11-((methylsulfonyl)oxy)-1,13-dioxo-2,3,6,7-tetrahydro-1H-3a,7-methanobenzo[g]pyrrolo[1,2-a][1,3]diazocine-4(5H)-carboxylate→N,N-Dimethylformamide dimethyl acetal
N,N-dimethylformamide+dimethyl sulfate→N,N-Dimethylformamide dimethyl acetal
2-acetylfuran→N,N-Dimethylformamide dimethyl acetal+(2E)-3-(Dimethylamino)-1-(2-furyl)prop-2-en-1-one

GC Analysis

Column type	Active phase	Temperature (°C)	Retention Index (I)	Temperature Control Method
Capillary	Polydimethyl siloxanes	-	726.	custom temperature program

Precursor

N,N-dimethylformamide
2-acetylfuran
methyl 2-((31S,6aR,9aR)-9-oxooctahydro-4H-pyrrolo[3,2,1-ij]quinolin-6a(31H)-yl)acetate
benzyl (3aR,7R)-7-(4-hydrazineyl-2,3-dimethoxyphenyl)-11-((methylsulfonyl)oxy)-1,13-dioxo-2,3,6,7-tetrahydro-1H-3a,7-methanobenzo[g]pyrrolo[1,2-a][1,3]diazocine-4(5H)-carboxylate

Downstream Product

4-(dimethylamino)-3-imidazo[1,2-a]pyridin-6-ylbut-3-en-2-one
3-(dimethylamino)-1-(2-hydroxyphenyl)prop-2-en-1-one
N-(3-cyanopyridin-2-yl)benzamide
1,1-Dimethylurea

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